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5-(Adamantan-1-yl)-3-anilinomethyl-2,3-dihydro-1,3,4-oxadiazole-2-thione
Journal article   Open access  Peer reviewed

5-(Adamantan-1-yl)-3-anilinomethyl-2,3-dihydro-1,3,4-oxadiazole-2-thione

Abdul-Malek S. Al-Tamimi, Omar A. Al-Deeb, Ali A. El-Emam, Seik Weng Ng and Edward R. T. Tiekink
Acta crystallographica. Section E, Crystallographic communications, Vol.69(5), pp.O729-o729
01/05/2013
DOI: https://doi.org/10.1107/S1600536813009835
PMID: 23723881

Abstract

Crystallography Physical Sciences Science & Technology
In the title compound, C19H23N3OS, the oxadiazole and benzene rings are inclined at a dihedral angle of 50.30 (11)degrees, with the major twist between them occurring at the ring-methylene N-C bond [N-N-C-N torsion angle = -101.2 (2)degrees]. In the crystal, helical supramolecular chains along [010] are sustained by N-H center dot center dot center dot S hydrogen bonds. These are linked into layers lying parallel to (101) by methylene-phenyl C-H center dot center dot center dot pi interactions.
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