Sign in
A Facile Synthesis of New Unsymmetrical Azines by Cyclodesulfurization Reactions of Dithioesters with Diamines
Journal article   Peer reviewed

A Facile Synthesis of New Unsymmetrical Azines by Cyclodesulfurization Reactions of Dithioesters with Diamines

S. M. Hassan
Phosphorus, sulfur, and silicon and the related elements, Vol.92(1-4), pp.213-217
01/07/1994

Abstract

Azines dithioester hydrazinecarbodithioate imidazoles pyrimidines thiosemicarbazones
Dithioesters 2a, b were prepared and methylated to give dimethyl thioesters 3a, b. Azines 4a-d and 5a, b were obtained in one step from 2 with primary diamines or in two steps through 3. Dithioesters 2a, b reacted with amines in ethanol to produce thiosemicarbazones 6a, b and 8a-d, while in butanol reacted with morpholine to form 7a, b

Metrics

1 Record Views

Details