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A Multicomponent One-pot Synthesis of 3-Cyanopyridine Derivatives
Journal article   Peer reviewed

A Multicomponent One-pot Synthesis of 3-Cyanopyridine Derivatives

Mohammed Al-Ghorbani, Moustafa A. Gouda and Jihan Qurban
INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, Vol.31(1), pp.77-80
01/03/2021

Abstract

Chemistry Chemistry, Organic Physical Sciences Science & Technology
A simple and efficient method was developed for synthesis of 2-amino-3-cyanopyridine and 3-cyanopyridine-2(1H)-ones (4a-e, 6a-e) from 2,6-dimethylheptan-4-one, aromatic aldehydes, and malononitrile or ethyl cyanoacetate in the presence of ammonium acetate in good to excellent yields and the structure of targets compounds was characterized by Fourier-transform infrared and H-1 and C-13 nuclear magnetic resonance and mass spectral and elemental analytical data.

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