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A New Asymmetric Photoisomerization of 2,3-Dihydropyrrolo[1,2-b]benzisothiazole 5,5-Dioxides
Journal article   Peer reviewed

A New Asymmetric Photoisomerization of 2,3-Dihydropyrrolo[1,2-b]benzisothiazole 5,5-Dioxides

Ibrahim Elghamry and Dietrich Doepp
Journal of the Korean Chemical Society, Vol.54(6), pp.727-730
20/12/2010

Abstract

Chemistry Chemistry, Multidisciplinary Physical Sciences Science & Technology
A tricyclic ring system bearing new stereogenic center namely 2,3-dihydro[1] benzothieno[3,2-b] pyrrole 4,4-dioxide was synthesized by asymmetric photoisomerization of 2,3-dihydropyrrolo[1,2-b] benzisothiazole 5,5-dioxide by irradiation with 245 nm emission of the low-pressure mercury lamp. The chemical structure and the purity of the photoproduct were delineated preliminarily by IR, NMR, and MS and finally confirmed by single crystal X-ray crystallography

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