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Cyclooctane Metathesis Catalyzed by Silica-Supported Tungsten Pentamethyl [( SiO)W(Me)(5)]: Distribution of Macrocyclic Alkanes
Journal article   Peer reviewed

Cyclooctane Metathesis Catalyzed by Silica-Supported Tungsten Pentamethyl [( SiO)W(Me)(5)]: Distribution of Macrocyclic Alkanes

Nassima Riache, Emmanuel Callens, Manoja K. Samantaray, Najeh M. Kharbatia, Muhammad Atiqullah and Jean-Marie Basset
Chemistry : a European journal, Vol.20(46), pp.15089-15094
10/11/2014
PMID: 25279445

Abstract

Chemistry Chemistry, Multidisciplinary Physical Sciences Science & Technology
Metathesis of cyclic alkanes catalyzed by the new surface complex [(SiO)W(Me)(5)] affords a wide distribution of cyclic and macrocyclic alkanes. The major products with the formula CnH2n are the result of either a ring contraction or ring expansion of cyclooctane leading to lower unsubstituted cyclic alkanes (5n7) and to an unprecedented distribution of unsubstituted macrocyclic alkanes (12n40), respectively, identified by GC/MS and by NMR spectroscopies.

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