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EFFICIENT SYNTHESIS OF NEW NITROGEN DONOR CONTAINING TRIPODS UNDER MICROWAVE IRRADIATION AND WITHOUT SOLVENT
Journal article   Peer reviewed

EFFICIENT SYNTHESIS OF NEW NITROGEN DONOR CONTAINING TRIPODS UNDER MICROWAVE IRRADIATION AND WITHOUT SOLVENT

Rachid Touzani, Abdelkrim Ramdani, Taibi Ben-Hadda, Sghir El Kadiri, Olivier Maury, Hubert Le Bozec and Pierre H. Dixneuf
Synthetic communications, Vol.31(9), pp.1315-1321
01/01/2001

Abstract

Five new N,N-bis(pyrazole-1-yl-methyl) alkylamines have been prepared in one step by condensation of two equivalents of 1-(hydroxymethyl)-3,5-disubstituted pyrazoles with a series of primary amines. This reaction is carried out under microwave irradiation (60 W) in the absence of solvent for 20 m and affords high yields (75-90%) of mixed nitrogen donor tripodal molecules.

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