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Efficient Synthesis of New Functionalized 2-(Hetaryl)thiazoles
Journal article   Peer reviewed

Efficient Synthesis of New Functionalized 2-(Hetaryl)thiazoles

Samir Bondock, Hossam El-Azab, Ez-Eldin M. Kandeel and Mohamed A. Metwally
Synthetic communications, Vol.43(1), pp.59-71
01/01/2013

Abstract

Japp-Klingmann phenyl isothiocyanate pyrazole pyridine thiazole
An efficient synthesis of the hitherto unknown ring system, 2-heteroaryl-thiazoles, is described via the reaction of 3-oxo-N-(4-phenylthiazol-2-yl)butanamide (1) with diazotized heterocyclic amine, phenyl isothiocyanate, dimethylformamide-dimethylacetal, and hydrazine hydrate, and the reaction of 2-chloro-N-(4-phenylthiazol-2-yl)acetamide (13) with some sulfur nucleophiles and malononitrile. The structures of the compounds prepared were determined by analytical and spectral analyses.

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