Abstract
In this article we describe uncomplicated and flexible method for the preparation of three-dimensional highly ordered mesoporous cobalt films containing close arranged arrays of spherical void of uniform size. Arranged mesoporous cobalt films were precisely prepared by electrodeposition of hexagonal H1-e Co ion using Brij -76 template. The electrodeposited mesopores films were described via various techniques such as electronic microscopy (SEM & TEM), low angle X-ray diffraction (XRD), cyclic voltammetric and chronoamperometric methods. The appropriateness of thin films as high - performance super capacitors electrode materials is indicated electrochemically using cyclic voltammetry (CV) technique. The initial stages of nucleation, growth mechanism of electrodeposition of Co was demonstrated via cyclic voltammetry and chronoamperometry tools.