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Lipase mediated resolution of gamma-azidoalcohols in aqueous and organic media: Synthesis of (R)- and (S)-fluoxetine and duloxetine
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Lipase mediated resolution of gamma-azidoalcohols in aqueous and organic media: Synthesis of (R)- and (S)-fluoxetine and duloxetine

Ahmed Kamal, M. Shaheer Malik, Ahmad Ali Shaik and Shaik Azeeza
Journal of molecular catalysis. B, Enzymatic, Vol.58(1-4), pp.132-137
01/06/2009

Abstract

Biochemistry & Molecular Biology Chemistry Chemistry, Physical Life Sciences & Biomedicine Physical Sciences Science & Technology
A simple and efficient method for the synthesis of optically active gamma-azidoalcohols is described. The lipase catalyzed kinetic resolutions of acetates of gamma-azidoalcohols in aqueous as well as organic media have been studied. The enantiomerically pure gamma-azidoalcohols obtained by the kinetic resolution in high enantiopurity have been utilized towards the synthesis of enantiomeric pairs of anti-depressant drugs, fluoxetine and duloxetine. (C) 2008 Elsevier B.V. All rights reserved.

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