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P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide
Journal article   Open access

P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide

Normen Peulecke, Bhaskar R. Aluri, Anina Woehl, Anke Spannenberg and Mohammed H. Al-Hazmi
Acta crystallographica. Section E, Structure reports online, Vol.65(5), pp.O1084-U2592
01/05/2009
PMID: 21583899

Abstract

Crystallography Physical Sciences Science & Technology
The title compound, C(24)H(30)N(2)P(2)S(2), was obtained by the reaction of Ph(2)PN(iPr)P(Ph)N(iPr)H with elemental sulfur in tetrahydrofuran. In the solid state, intramolecular N-H center dot center dot center dot S hydrogen bonding influences the molecular conformation; a P-N-P-N torsion angle of 2.28 (9)degrees is observed. The two phenyl rings attached to one P atom form a dihedral angle of 74.02 (4)degrees.
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https://doi.org/10.1107/S1600536809014238View
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