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Pd(OAc)(2)-CATALYZED CARBONYLATIVE COUPLING OF ARYL IODIDE WITH ORTHO-HALOAMINES IN WATER
Journal article   Peer reviewed

Pd(OAc)(2)-CATALYZED CARBONYLATIVE COUPLING OF ARYL IODIDE WITH ORTHO-HALOAMINES IN WATER

Pawan J. Tambade, Yogesh P. Patil, Ziyauddin S. Qureshi, Kishor P. Dhake and Bhalchandra M. Bhanage
Synthetic communications, Vol.42(2), pp.176-185
01/01/2012

Abstract

Chemistry Chemistry, Organic Physical Sciences Science & Technology
The carbonylative cross coupling of aryl iodide with ortho-haloaniline to ortho-haloanilide using phosphine-free Pd(OAc)(2) catalyst in water as a reaction medium has been studied. The present protocol facilitated the reaction of o-haloanilines with a wide variety of hindered and functionalized aryl iodides, affording good yields of the desired products. The protocol was also extended for the synthesis of benzoxazoles through cyclization of ortho-haloanilide using Cu(acac)(2) catalyst.

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