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Poly(ester-amide)s Derived From Adipic Acid, 1,4-Butanediol and β-Alanine: Synthesis and Characterization
Journal article   Peer reviewed

Poly(ester-amide)s Derived From Adipic Acid, 1,4-Butanediol and β-Alanine: Synthesis and Characterization

Marwa Abbes, Slim Salhi, Lénaïg Lefevre, Christelle Delaite, Souhir Abid and Rachid El Gharbi
Journal of macromolecular science. Part A, Pure and applied chemistry, Vol.52(1), pp.56-63
02/01/2015

Abstract

melt polycondensation Poly(esteramide) thermal properties β-alanine
A series of polyesteramides (PEAs) differing in their amide/ester ratio, within a range of molar composition from 90/10 to 10/90, have been synthesized by a direct melt polycondensation of 1,4-butanediol, adipic acid and β-alanine. Their structure was fully characterized by FTIR and NMR spectroscopy. The resulting copolymers are amorphous, they are thermally stable to temperatures up to 330°C, and present increasing glass transition temperatures at increasing amide content.

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