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Rubber Chemicals Derived from Conjugate Addition. I. Syntheses of Novel 2-Thio-5-Amino Substituted Benzoquinones
Journal article   Peer reviewed

Rubber Chemicals Derived from Conjugate Addition. I. Syntheses of Novel 2-Thio-5-Amino Substituted Benzoquinones

Alan R. Katritzky, Herman H. Odens, Michael V. Voronkov, Charles J. Rostek and Otto W. Maender
Rubber chemistry and technology, Vol.74(5), pp.915-925
01/11/2001

Abstract

Abstract Alkylthio-substituted benzoquinones were prepared from benzoquinone and mercaptans in 50–94% yields via NaIO4 oxidation of the intermediate hydroquinones. Subsequent addition of primary and secondary amines, in the presence of air as an oxidizing agent, gave a range of 2-thio-5-amino-substituted benzoquinones. No oxidation at sulfur was detected under the described conditions.

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