SYNTHESIS, SPECTROSCOPIC STUDIES, AND X-RAY CRYSTAL STRUCTURE OF N-HETERYLIMINOPHOSPHORANES

H. Z. Alkhathlan; M. A. Al-Jaradah; K. A. Al-Farhan; A. A. Mousa

doi:10.1080/10426500490262513

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SYNTHESIS, SPECTROSCOPIC STUDIES, AND X-RAY CRYSTAL STRUCTURE OF N-HETERYLIMINOPHOSPHORANES

Journal article

Peer reviewed

SYNTHESIS, SPECTROSCOPIC STUDIES, AND X-RAY CRYSTAL STRUCTURE OF N-HETERYLIMINOPHOSPHORANES

H. Z. Alkhathlan, M. A. Al-Jaradah, K. A. Al-Farhan and A. A. Mousa

Phosphorus, sulfur, and silicon and the related elements, Vol.179(2), pp.373-388

01/02/2004

DOI: https://doi.org/10.1080/10426500490262513

Abstract

2-Aminoacetophenone

acid anhydrides

azides

iminophosphoranes

quinoline

N-[2-(α-Bromoacetyl)phenyl]imides (prepared in two steps from 2-aminoacetophenone) gave, upon treatment with sodium azide, fused azidoquinolines via an intramolecular cyclization. Reaction of the above azides with phosphines gave N-heteryliminophosphoranes. The IR, 1 H-, 13 C-, and 31 P-NMR and MS spectra of these compounds as well as the x-ray crystal structure of two of them is reported.

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Title: SYNTHESIS, SPECTROSCOPIC STUDIES, AND X-RAY CRYSTAL STRUCTURE OF N-HETERYLIMINOPHOSPHORANES
Creators - without role: H. Z. Alkhathlan - King Saud University
M. A. Al-Jaradah - King Saud University
K. A. Al-Farhan - King Saud University
A. A. Mousa - King Saud University
Publication Details: Phosphorus, sulfur, and silicon and the related elements, Vol.179(2), pp.373-388
Publisher: Taylor & Francis Group
Identifiers: 9948639208331
Academic Unit: King Saud University
Language: English
Resource Type: Journal article