Sonochemical synthesis and fabrication of neodymium sesquioxide entrapped with graphene oxide based hierarchical nanocomposite for highly sensitive electrochemical sensor of anti-cancer (raloxifene) drug

Tse-Wei Chen; Johnson Princy Merlin; Shen-Ming Chen; Sathiyan Anandaraj; Mohamed S. Elshikh; Tien-Wen Tseng; Kang Wang; Dongdong Qi; Jianzhuang Jiang; Mohammad Suliman El-Shikh

doi:10.1016/j.ultsonch.2019.104717

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Sonochemical synthesis and fabrication of neodymium sesquioxide entrapped with graphene oxide based hierarchical nanocomposite for highly sensitive electrochemical sensor of anti-cancer (raloxifene) drug

Journal article

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Sonochemical synthesis and fabrication of neodymium sesquioxide entrapped with graphene oxide based hierarchical nanocomposite for highly sensitive electrochemical sensor of anti-cancer (raloxifene) drug

Tse-Wei Chen, Johnson Princy Merlin, Shen-Ming Chen, Sathiyan Anandaraj, Mohamed S. Elshikh, Tien-Wen Tseng, Kang Wang, Dongdong Qi, Jianzhuang Jiang and Mohammad Suliman El-Shikh

Ultrasonics sonochemistry, Vol.64, pp.104717-104717

01/06/2020

DOI: https://doi.org/10.1016/j.ultsonch.2019.104717

PMID: 32062532

Abstract

Acoustics

Chemistry

Chemistry, Multidisciplinary

Physical Sciences

Science & Technology

Technology

The ultrasound-assisted synthesis of a novel neodymium sesquioxide nanoparticles (Nd2O5 NPs) decorated graphene oxide (GO) nanocomposite under ultrasonic probe (Ultrasonic processor model-PR 1000; frequency-30 kHz; power of 100 W/cm(2) ) has been reported. After then, SEM, TEM, XRD, EDX and electrochemical impedance spectroscopy characterized was analyzed using Nd2O5 NPs@GO nanomaterial. Furthermore, the nanomaterial modified GCE (glassy carbon electrode) shows excellent electrochemical sensing performance towards anti-cancer drug. Raloxifene is one of the important anti-cancer drug. Moreover, the fabricated electrochemical sensor has showed a wide linear range for raloxifene between 0.03 and 472.5 mu M and nanomolar detection limit (18.43 nM). In addition, the Nd2O5 NPs@GO modified sensor has been applied to the determination of raloxifene in human blood and urine samples.

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Title: Sonochemical synthesis and fabrication of neodymium sesquioxide entrapped with graphene oxide based hierarchical nanocomposite for highly sensitive electrochemical sensor of anti-cancer (raloxifene) drug
Creators - without role: Tse-Wei Chen - Natl Taipei Univ Technol, Dept Chem Engn & Biotechnol, 1,Sect 3,Chung Hsiao East Rd, Taipei 106, Taiwan
Johnson Princy Merlin - Bishop Heber Coll, Dept Chem, Tiruchirappalli, Tamil Nadu, India
Shen-Ming Chen - National Taipei University of Technology
Sathiyan Anandaraj - Bishop Heber Coll, Dept Chem, Tiruchirappalli, Tamil Nadu, India
Mohamed S. Elshikh - King Saud University
Tien-Wen Tseng - National Taipei University of Technology
Kang Wang - University of Science and Technology Beijing
Dongdong Qi - University of Science and Technology Beijing
Jianzhuang Jiang - University of Science and Technology Beijing
Mohammad Suliman El-Shikh - King Saud University
Publication Details: Ultrasonics sonochemistry, Vol.64, pp.104717-104717
Publisher: Elsevier
Number of pages: 8
Grant note: MOST 107-2113-M-027-005-MY3 / Ministry of Science and Technology, Taiwan NTUT-USTB-108-12; TW2019008 / National Taipei University of Technology King Saud University, Deanship of Scientific Research, College of Science, Research Center; King Saud University 21631003; 21671017; 21871024 / Natural Science Foundation of China; National Natural Science Foundation of China (NSFC) FRF-BD-17-016A / Fundamental Research Funds for the Central Universities of China; Fundamental Research Funds for the Central Universities NTUT-USTB-108-12; TW2019008 / University of Science and Technology Beijing
Identifiers: 9948424408331
Academic Unit: King Saud University
Language: English
Resource Type: Journal article