Abstract
A combination of x-ray diffraction analysis, with mechanical testing in tension and bending has been used to investigate he metallurgical structures and mechanical properties for as-received and heat-treated stainless steel orthodontic wires. Two different proprietary wire types were selected, having a wide range in cross-sectional dimensions: 0.016- 0.030-, and 0.050- or 0.051-inch diameters, and 0.017 × 0.025-inch rectangular specimens. Heat treatments were performed for 10 minutes in air at temperatures of 700°, 900°, and 1100° F. The x-ray diffraction patterns showed that the as-received 0.016-inch diameter and 0.017 × 0.025-inch wires of both proprietary types consisted of a two-phase structure containing a martensitic phase along with the austenitic phase. This duplex structure was converted entirely to austenite with heat treatment for one wire type, but persisted after heat treatment for the other wire type. The largest diameter, 0.050- or 0.051-inch, wires of both types were single-phase austenitic structure for both the as-received and heat-treated conditions. Evidence of substantial preferred crystallographic orientation or texturing in these orthodontic wires was also found by x-ray diffraction. As in our previous studies, the modulus of elasticity in bending was significantly less than the value obtained in tension for only the smaller cross-sectional wires. The 0.05 radian flexural yield strength correlated more closely with the 0.2% offset yield strength in tension than with the yield strength for 0.05% and 0.1% permanent. offsets.