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Synthesis, Crystal Structure, and Spectral Study of a Novel ndenoimidazole Carboxylic Acid Amide
Journal article   Peer reviewed

Synthesis, Crystal Structure, and Spectral Study of a Novel ndenoimidazole Carboxylic Acid Amide

R. M. Ghalib, S. H. Mehdi, A. M. Malla, M. G. Alam, A. K. Gupta, H. A. H. Alzahrani and S. B. Novakovic
Russian journal of organic chemistry, Vol.57(12), pp.2018-2023
01/12/2021

Abstract

Chemistry Chemistry, Organic Physical Sciences Science & Technology
3a,8a-Dihydroxy-2,8-dioxo-1,3a,8,8a-tetrahydro-2H-indeno[1,2-d]imidazole-3-carboxamide has been synthesized in 85% yield from ninhydrin and biuret via a green facile procedure that is free of workup and column chromatography. The product structure has been established based on FT-IR, NMR, and mass spectra and finally confirmed by single crystal X-ray analysis. The compound crystalized as monoclinic colorless plates with P2(1)/c space group.

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