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Synthesis and Characterization of Privileged Monodentate Phosphoramidite Ligands and Chiral Bronsted Acids Derived from D-Mannitol
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Synthesis and Characterization of Privileged Monodentate Phosphoramidite Ligands and Chiral Bronsted Acids Derived from D-Mannitol

Abdullah Mohammed A. Al-Majid, Assem Barakat, Yahia Nasser Mabkhot and Mohammad Shahidul Islam
International journal of molecular sciences, Vol.13(3), pp.2727-2743
01/03/2012
PMCID: PMC3317684
PMID: 22489121

Abstract

Biochemistry & Molecular Biology Chemistry Chemistry, Multidisciplinary Life Sciences & Biomedicine Physical Sciences Science & Technology
The synthesis of several novel chiral phosphoramidite ligands (L1-L8) with C-2 symmetric, pseudo C-2 symmetric secondary amines and chiral Bronsted acids 1a,b has been achieved. These chiral auxiliaries were obtained from commercially available D-mannitol, and secondary amines in moderate to excellent yields. Excellent diastereoselectivites of ten chiral auxiliaries were obtained. The chiral phosphoramidite ligands and chiral Bronsted acids were fully characterized by spectroscopic methods.
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https://doi.org/10.3390/ijms13032727View
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