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Synthesis and Crystal Structures of Benzimidazole-2-thione Derivatives by Alkylation Reactions
Journal article   Open access  Peer reviewed

Synthesis and Crystal Structures of Benzimidazole-2-thione Derivatives by Alkylation Reactions

Sayed H. El Ashry, Yeldez El Kilany, Nariman M. Nahas, Assem Barakat, Nadia Al-Qurashi, Hazem A. Ghabbour and Hoong-Kun Fun
Molecules (Basel, Switzerland), Vol.21(1), pp.E12-E12
22/12/2015
DOI: https://doi.org/10.3390/molecules21010012
PMCID: PMC6273855
PMID: 26703551

Abstract

Biochemistry & Molecular Biology Chemistry Chemistry, Multidisciplinary Life Sciences & Biomedicine Physical Sciences Science & Technology
Alkylated, benzylated and bromoalkylated benzimidazole-thione that intramolecularly heterocyclized to 3,4-dihydro-2H-[1,3]thiazino[3,2-a]benzimidazole were synthesized. The chemical structure of the synthesized product was characterized by Infra Red, H-1-NMR, C-13-NMR, and Mass spectroscopy. Furthermore, the molecular structures of 8 and 9 were confirmed by X-ray single crystallography in different space groups, Pbca and P2(1)/c, respectively.
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https://doi.org/10.3390/molecules21010012View
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