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Synthesis of bishomobenzoctamine 2-(9,10-dihydro-9,10-propanoanthracen-9-yl)-N-methylethanamine
Journal article   Peer reviewed

Synthesis of bishomobenzoctamine 2-(9,10-dihydro-9,10-propanoanthracen-9-yl)-N-methylethanamine

Usama Karama, Adel Al-Saidey and Abdel Rahman Almansour
Journal of chemical research, Vol.2010(5), pp.241-242
01/05/2010
DOI: https://doi.org/10.3184/030823410X12715108891565

Abstract

Chemistry Chemistry, Multidisciplinary Physical Sciences Science & Technology
Tetracyclic bishomobenzoctamine as a homologue of benzoctamine 1 was synthesised. The key intermediate 9-(prop-2-en-1-yl)-9,10-dihydro-9,10-propanoanthracen-12-one was successfully synthesised via [3+4] cycloaddition of tetrabromoacetone on 9-allylanthracene by using ultrasonication at 15-20 degrees C followed by debromination.

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